SPECTROMETRIC IDENTIFICATION OF ORGANIC COMPOUNDS, 6TH ED

Author: Robert Silverstein & Francis Webster

Publisher: John Wiley & Sons

ISBN: 9788126509720

Category: Chemistry

Page: 496

View: 1706

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Market_Desc: Organic and Analytical in the Forensics, Chemical and Pharmaceutical Industries Special Features: · A how-to, hands-on teaching manual· Considerably expanded NMR coverage--NMR spectra can now be interpreted in exquisite detail· New chapters on correlation NMR spectrometry (2-D NMR) and spectrometry of other important nuclei· Uses a problem-solving approach with extensive reference charts and tables· An extensive set of real-data problems offers a challenge to the practicing chemist About The Book: The book provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry.
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Undergraduate Instrumental Analysis, Sixth Edition

Author: James W. Robinson,Eileen M. Skelly Frame,George M. Frame II

Publisher: CRC Press

ISBN: 9780849306501

Category: Science

Page: 1079

View: 1895

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Completely rewritten, revised, and updated, this Sixth Edition reflects the latest technologies and applications in spectroscopy, mass spectrometry, and chromatography. It illustrates practices and methods specific to each major chemical analytical technique while showcasing innovations and trends currently impacting the field. Many of the chapters have been individually reviewed by teaching professors and include descriptions of the fundamental principles underlying each technique, demonstrations of the instrumentation, and new problem sets and suggested experiments appropriate to the topic. About the authors... JAMES W. ROBINSON is Professor Emeritus of Chemistry, Louisiana State University, Baton Rouge. A Fellow of the Royal Chemical Society, he is the author of over 200 professional papers and book chapters and several books including Atomic Absorption Spectroscopy and Atomic Spectroscopy. He was Executive Editor of Spectroscopy Letters and the Journal of Environmental Science and Health (both titles, Marcel Dekker, Inc.) and the Handbook of Spectroscopy and the Practical Handbook of Spectroscopy (both titles, CRC Press). He received the B.Sc. (1949), Ph.D. (1952), and D.Sc. (1978) degrees from the University of Birmingham, England. EILEEN M. SKELLY FRAME recently was Clinical Assistant Professor and Visiting Research Professor, Rensselaer Polytechnic Institute, Troy, New York. Dr. Skelly Frame has extensive practical experience in the use of instrumental analysis to characterize a wide variety of substances, from biological samples and cosmetics to high temperature superconductors, polymers, metals, and alloys. Her industrial career includes supervisory roles at GE Corporate Research and Development, Stauffer Chemical Corporate R&D, and the Research Triangle Institute. She is a member of the American Chemical Society, the Society for Applied Spectroscopy, and the American Society for Testing and Materials. Dr. Skelly Frame received the B.S. degree in chemistry from Drexel University, Philadelphia, Pennsylvania, and the Ph.D. in analytical chemistry from Louisiana State University, Baton Rouge. GEORGE M. FRAME II is Scientific Director, Chemical Biomonitoring Section of the Wadsworth Laboratory, New York State Department of Health, Albany. He has a wide range of experience in the field and has worked at the GE Corporate R&D Center, Pfizer Central Research, the U.S. Coast Guard R&D Center, the Maine Medical Center, and the USAF Biomedical Sciences Corps. He is an American Chemical Society member. Dr. Frame received the B.A. degree in chemistry from Harvard College, Cambridge, Massachusetts, and the Ph.D. degree in analytical chemistry from Rutgers University, New Brunswick, New Jersey.
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Introduction to Organic Laboratory Techniques

A Small Scale Approach

Author: Donald L. Pavia,Gary M. Lampman,George S. Kriz,Randall G. Engel

Publisher: Cengage Learning

ISBN: 0534408338

Category: Science

Page: 1028

View: 524

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Featuring 66 experiments, detailing 29 techniques, and including several explicating essays, this lab manual covers basic lab techniques, molecular modeling, properties and reactions of organic compounds, the identification of organic substances, project-based experiments, and each step of the various techniques. The authors teach at Western Washington University and North Seattle Community College. Annotation ♭2004 Book News, Inc., Portland, OR (booknews.com).
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Spectroscopy of Organic Compounds

Author: P S Kalsi

Publisher: New Age International

ISBN: 9788122415438

Category: Chemistry, Organic

Page: 652

View: 6055

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The Sixth Edition Of This Widely Used Text Includes New Examples / Spectra / Explanations / Expanded Coverage To Update The Topic Of Spectroscopy. The Artwork And Material In All Chapters Has Been Revised Extensively For Students Understanding.New To This Edition * New Discussion And New Ir, 1H Nmr, 13C Nmr And Ms Spectra. * More Important Basic Concepts Highlighted And Put In Boxes Throughout This Edition. * Chapters On 1H Nmr And 13C Nmr Rewritten And Enlarged. More On Cosy, Hetcor, Dept And Inadequate Spectra. * A Rational Approach For Solving The Structures Via Fragmentation Pathways In Ms. * Increased Power Of The Book By Providing Further Extensive Learning Material In This Revised Edition. * A Quick And An Easy Access To Topics In Ugc Model Curricula.With Its Comprehensive Coverage And Systematic Presentation The Book Would Serve As An Excellent Text For B.Sc. (Hons.) And M.Sc. Chemistry Students. It Provides Knowledge To Excel At Any Level, University Examination, Competitive Examinations E.G. Net And Before Interview Boards.
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Chemistry of Plant Natural Products

Stereochemistry, Conformation, Synthesis, Biology, and Medicine

Author: Sunil Kumar Talapatra,Bani Talapatra

Publisher: Springer

ISBN: 3642454100

Category: Science

Page: 1180

View: 6923

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Aimed at advanced undergraduate and graduate students and researchers working with natural products, Professors Sunil and Bani Talapatra provide a highly accessible compilation describing all aspects of plant natural products. Beginning with a general introduction to set the context, the authors then go on to carefully detail nomenclature, occurrence, isolation, detection, structure elucidation (by both degradation and spectroscopic techniques) stereochemistry, conformation, synthesis, biosynthesis, biological activity and commercial applications of the most important natural products of plant origin. Each chapter also includes detailed references (with titles) and a list of recommended books for additional study making this outstanding treatise a useful resource for teachers of chemistry and researchers working in universities, research institutes and industry.
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Spectrometric identification of organic compounds

Author: Robert Milton Silverstein,Francis X. Webster

Publisher: John Wiley & Sons

ISBN: N.A

Category: Science

Page: 482

View: 1798

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This book is characterized by its problem-solving approach with extensive reference charts and tables. First published in 1962, this was the first book on the identification of organic compounds using spectroscopy. Now considered a classic, it can be found on the shelf of every Organic Chemist. The key strength of this text is the extensive set of real-data problems in Chapters 8 and 9. Even professional chemists use these spectra as reference data. Spectrometric Identification of Organic Compounds is written by and for organic chemists, and emphasizes the synergistic effect resulting from the interplay of the spectra.
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Microscale Operational Organic Chemistry

A Problem-solving Approach to the Laboratory Course

Author: John W. Lehman

Publisher: Prentice Hall

ISBN: N.A

Category: Science

Page: 844

View: 9490

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This practical guide to the core operations in the organic lab gives an excellent selection of clever microscale experiments, enabling users to have an excellent resource that encourages scientific problem-solving. The unique problem-solving approach given in this guide encourages readers to master major lab operations, explaining why they are carried out the way they are. Readers will understand each scientific problem, formulate a meaningful hypothesis, and then solve the problem. Sections on qualitative organic analysis and basic operations such as glassware use, conducting chemical reactions, washing and drying operations, purification operations, measuring, and instrumental analyses round out this handy reference work. The extensive appendices, bibliography, and basic operations sections make this an excellent desktop resource for organic chemists and other lab technicians.
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The student's lab companion

laboratory techniques for organic chemistry : standard scale and microscale

Author: John W. Lehman

Publisher: Pearson College Div

ISBN: N.A

Category: Science

Page: 388

View: 1434

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This comprehensive lab companion provides a thorough introduction to all of the significant operations used in the organic lab, for both traditional-scale and microscale applications. It includes enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. lab.Makes substantive revisions of many operations to clarify existing material and add new information. Emphasizes environmentally friendly (i.e. green ) lab experiments. Adds a new section on Chemistry and the Environment.A useful guide for chemists and other professionals who do laboratory work in the scientific fields.
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Operational Organic Chemistry

A Problem-solving Approach to the Laboratory Course

Author: John W. Lehman

Publisher: N.A

ISBN: N.A

Category: Science

Page: 808

View: 3109

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This traditional-scale lab book prepares readers to perform the fundamental operations of organic chemistry in the laboratory and apply the operations intelligently in new situations -- to think and act like an organic chemist. Features traditional-scale laboratory procedures which do not require expensive, special glassware and which provide enough material for visual and physical characterization. Contains 115 experiments -- 12 experiments that teach basic operations, 46 experiments that reinforce concepts, and 47 minilabs (shorter experiments that can be used to fill partial or shorter lab periods). Features many experiments that use common or household compounds. Provides a section on qualitative organic analysis. Includes sections on using the chemical literature, keeping a notebook, and planning a synthesis. For anyone interested in organic chemistry.
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Experimental Organic Chemistry

A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Brooks/Cole Publishing Company

ISBN: N.A

Category: Science

Page: 927

View: 8205

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This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.
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