Experimental Organic Chemistry

Laboratory Manual

Author: Joaquín Isac-García,José A. Dobado,Francisco G. Calvo-Flores,Henar Martínez-García

Publisher: Academic Press

ISBN: 0128039353

Category: Science

Page: 500

View: 408

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Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. Organizes lab course coverage in a logical and useful way Features a valuable chapter on Green Chemistry Experiments Includes 84 experiments arranged according to increasing complexity
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Experimental Organic Chemistry: A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Cengage Learning

ISBN: 1305687876

Category: Science

Page: 960

View: 1602

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Perform chemistry experiments with skill and confidence in your organic chemistry lab course with this easy-to-understand lab manual. EXPERIMENTAL ORGANIC CHEMISTRY: A MINISCALE AND MICROSCALE APPROACH, Sixth Edition first covers equipment, record keeping, and safety in the laboratory, then walks you step by step through the laboratory techniques you'll need to perform all experiments. Individual chapters show you how to use the techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. New experiments in Chapter 17 and 18 demonstrate the potential of chiral agents in fostering enantioselectivity and of performing solvent-free reactions. A bioorganic experiment in Chapter 24 gives you an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
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Experimental Organic Chemistry

A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Brooks/Cole Publishing Company

ISBN: N.A

Category: Science

Page: 927

View: 2122

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This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.
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Experimental Organic Chemistry

Author: Philippa B. Cranwell,Laurence M. Harwood,Christopher J. Moody

Publisher: John Wiley & Sons

ISBN: 1119952387

Category: Science

Page: 688

View: 697

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Previous edition by Laurence M. Harwood, Christopher J. Moody, and Jonathan M. Percy.
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Experimental Organic Chemistry: A Miniscale and Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Cengage Learning

ISBN: 1439049149

Category: Science

Page: 960

View: 1076

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Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first covers equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
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Organic Chemistry

A Laboratory Manual

Author: Syed Mumtazuddin

Publisher: Alpha Science International Limited

ISBN: 9781842658123

Category: Science

Page: 300

View: 866

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ORGANIC CHEMISTRY: A Laboratory Manual includes basic experimental techniques, some important organic preparations, principles and experiments in chromatography, detection of organic compounds and mixtures, isolation of some natural products, and quantitative estimation of some organic compounds. Without compromising with the quality of subject matter, the language of the book has been deliberately kept simple and easy to follow. This book will guide the student to detect the compound with ease by performing the experiments step by step in a systematic manner. The book contains complete theory, reasoning and reactions involved in each experiment. An illustration has been provided to teach the students how to write the identification experiment. Experiments on the determination of COD, DO and BOD have been lucidly described with their principles. Appendix provides list of hazardous chemicals and their effects, safety measures to be observed in laboratory, first aid in the case of laboratory accidents, etc.
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Experimental Organic Chemistry

A Balanced Approach, Macroscale and Microscale

Author: Jerry R. Mohrig

Publisher: W H Freeman & Company

ISBN: 9780716733300

Category: Science

Page: 733

View: 8131

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This laboratory manual seeks to provide a balance between the approaches of microscale and macroscale.
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