Experimental Organic Chemistry

Laboratory Manual

Author: Joaquín Isac-García,José A. Dobado,Francisco G. Calvo-Flores,Henar Martínez-García

Publisher: Academic Press

ISBN: 0128039353

Category: Science

Page: 500

View: 3447

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Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. Organizes lab course coverage in a logical and useful way Features a valuable chapter on Green Chemistry Experiments Includes 84 experiments arranged according to increasing complexity
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Experimental Organic Chemistry: A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Cengage Learning

ISBN: 1305687876

Category: Science

Page: 960

View: 2134

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Perform chemistry experiments with skill and confidence in your organic chemistry lab course with this easy-to-understand lab manual. EXPERIMENTAL ORGANIC CHEMISTRY: A MINISCALE AND MICROSCALE APPROACH, Sixth Edition first covers equipment, record keeping, and safety in the laboratory, then walks you step by step through the laboratory techniques you'll need to perform all experiments. Individual chapters show you how to use the techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. New experiments in Chapter 17 and 18 demonstrate the potential of chiral agents in fostering enantioselectivity and of performing solvent-free reactions. A bioorganic experiment in Chapter 24 gives you an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
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Experiments in Organic Chemistry

A Laboratory Manual Designed to Accompany Outlines of Organic Chemistry

Author: Forris Jewett Moore,Henry Weeden Underwood

Publisher: N.A

ISBN: N.A

Category: Chemistry, Organic

Page: 133

View: 6467

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Laboratory Manual of Organic Chemistry

Author: Raj K. Bansal

Publisher: New Age International

ISBN: 8122424740

Category: Chemistry

Page: 304

View: 636

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About the Book: The manual has been thoroughly revised, several new experiments and tests have been added while some redundant material has been deleted. Chapter 2 has been completely rewritten. An obvious change of this edition constitutes the splitting of Chapter 7 into two separate Chapters. Tables on derivatives of organic compounds have been expended. Also included are 20 estimations, 75 preparations and isolation experiments and approximately 135 in-text questions related to the experiments. The approximation of modern spectroscopic techniques to structure determination have been discussed in the last Chapter. This book is designed both for undergraduate and postgraduate level students with its enhanced and comprehensive presentation. This is an indispensable book for organic chemistry practicals. About the Author: Dr. Raj K. Bansal received his M.S. from the University of California, Davis, Calif, U.S.A., and Ph.D. from Calgary University, Calgary, Alberta, Canada. He was a postdoctoral fellow at the National Research Council (N.R.C.) of Canada in Halifax, N.S., Canada, followed by a Research Associateship at the Mellon Institute of Science, Carnegie-Mellon University, Pittsburgh Pa., U.S.A. Dr. Bansal has published a number of research papers in various foreign and Indian scientific journals. He is the author of six books on chemistry including this work-A Textbook of Organic Chemistry (5th ed., 2007), Organic Chemistry-Problems and Solutions (2nd edn., 2006), and Heterocyclic Chemistry (4th edn., 2005). One of his books, Synthetic Approaches in Organic Chemistry has been reprinted by Jones and Bartlett Publishers, Sudbury, Massachusetts, U.S.A. Dr. Bansal was a former Professor, Department of Chemistry, Indian Institute of Technology, Delhi, Hauz Khas, New Delhi.
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Organic Chemistry

A Laboratory Manual

Author: Syed Mumtazuddin

Publisher: Alpha Science International Limited

ISBN: 9781842658123

Category: Science

Page: 300

View: 4412

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ORGANIC CHEMISTRY: A Laboratory Manual includes basic experimental techniques, some important organic preparations, principles and experiments in chromatography, detection of organic compounds and mixtures, isolation of some natural products, and quantitative estimation of some organic compounds. Without compromising with the quality of subject matter, the language of the book has been deliberately kept simple and easy to follow. This book will guide the student to detect the compound with ease by performing the experiments step by step in a systematic manner. The book contains complete theory, reasoning and reactions involved in each experiment. An illustration has been provided to teach the students how to write the identification experiment. Experiments on the determination of COD, DO and BOD have been lucidly described with their principles. Appendix provides list of hazardous chemicals and their effects, safety measures to be observed in laboratory, first aid in the case of laboratory accidents, etc.
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Experimental Organic Chemistry

Author: Philippa B. Cranwell,Laurence M. Harwood,Christopher J. Moody

Publisher: John Wiley & Sons

ISBN: 1119952387

Category: Science

Page: 688

View: 1798

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Previous edition by Laurence M. Harwood, Christopher J. Moody, and Jonathan M. Percy.
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Experimental Organic Chemistry

A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Brooks/Cole Publishing Company

ISBN: N.A

Category: Science

Page: 927

View: 6802

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This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.
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Laboratory Manual

Containing Directions for a Course of Experiments in Organic Chemistry, Systematically Arranged to Accompany Remsen's Organic Chemistry, Revision of 1992 (Classic Reprint)

Author: W. R. Orndorff

Publisher: N.A

ISBN: 9781330764114

Category: Science

Page: 186

View: 598

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Excerpt from Laboratory Manual: Containing Directions for a Course of Experiments in Organic Chemistry, Systematically Arranged to Accompany Remsen's Organic Chemistry, Revision of 1992 The student is expected to be familiar with the General Part of Gatterman's Practical Methods of Organic Chemistry, translated by Schober and Babasinian, 3d American Edition, pages 1 to 77. Descriptions of the methods used in the Laboratory of Organic Chemistry will be found in this part of the book. Before beginning any experiment the student is expected to read carefully the directions given in the Laboratory Manual for that experiment and to be sure that he understands them. If in doubt about any point he should consult the instructor or the assistant before beginning the experiment. He is urged to read ahead of the experiment he is doing, when opportunity presents itself, and he will find that it is frequently possible to be carrying on two or more experiments at the same time. It is necessary to use every minute in the laboratory to advantage in order to finish the required work in the allotted time. When the apparatus required for the experiment has been set up according to the directions given in the manual the student requests the assistant in charge of his section in the laboratory to inspect it. If the apparatus is satisfactory the student may begin the work. If it is not satisfactory the assistant will indicate what changes are necessary. The experiment is then performed by the student and the results are inspected by the assistant. Thus each experiment is checked at the beginning and at the end by the assistant, who also watches the student while the experiment is in progress. If the method of procedure is not correct or could be bettered, the student is at once informed of it. About the Publisher Forgotten Books publishes hundreds of thousands of rare and classic books. Find more at www.forgottenbooks.com This book is a reproduction of an important historical work. Forgotten Books uses state-of-the-art technology to digitally reconstruct the work, preserving the original format whilst repairing imperfections present in the aged copy. In rare cases, an imperfection in the original, such as a blemish or missing page, may be replicated in our edition. We do, however, repair the vast majority of imperfections successfully; any imperfections that remain are intentionally left to preserve the state of such historical works.
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