Annual Reports on NMR Spectroscopy

Author: Graham A. Webb

Publisher: Academic Press

ISBN: 0123970202

Category: Science

Page: 362

View: 959

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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.
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Applications of Physical Methods to Inorganic and Bioinorganic Chemistry

Author: Robert A. Scott,Charles M. Lukehart

Publisher: John Wiley & Sons

ISBN: 1118625285

Category: Science

Page: 592

View: 3468

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Modern spectroscopic and instrumental techniques are essential tothe practice of inorganic and bioinorganic chemistry. This firstvolume in the new Wiley Encyclopedia of Inorganic ChemistryMethods and Applications Series provides a consistent andcomprehensive description of the practical applicability of a largenumber of techniques to modern problems in inorganic andbioinorganic chemistry. The outcome is a text that providesinvaluable guidance and advice for inorganic and bioinorganicchemists to select appropriate techniques, whilst acting as asource to the understanding of these methods. This volume is also available as part of Encyclopedia ofInorganic Chemistry, 5 Volume Set. This set combines all volumes published as EIC Books from 2007to 2010, representing areas of key developments in the field ofinorganic chemistry published in the Encyclopedia of InorganicChemistry. ahref="http://eu.wiley.com/WileyCDA/WileyTitle/productCd-1119994284.html"Findout more/a.
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200 and More NMR Experiments

Author: Stefan Berger,Siegmar Braun

Publisher: Wiley-VCH

ISBN: 9783527310678

Category: Science

Page: 854

View: 343

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This work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein: ? Which experiment can best yield the desired information? ? How must the chosen experiment be performed? ? How does one read the required information from the spectrum? ? How does this particular pulse sequence work? ? Which other experiments give similar information? This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin with 76 amino acids. What is new in this third edition? 1. 24 new experiments have been inserted into the 14 chapters that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET, DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved HMBC, (1,1)- and (1,n)-ADEQUATE, STD, REDOR, and HR-MAS. 2. 20 new protein NMR experiments have been specially devised and are collected in the newly added Chapter 15, ProteinNMR, for which one needs a special model sample: fully 13C- and 15N-labeled human ubiquitin. Techniques used include the constant time principle, the PEP method, filters, gradient selection, and the echo/anti-echo procedure. The guide has been written by experts in this field, following the principle of learning by doing: all the experiments have been specially performed for this book, exactly as described and shown in the spectra that are reproduced. Being a reference source and work-book for the NMR laboratory as well as a textbook, it is a must for every scientist working with NMR, as well as for students preparing for their laboratory courses
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Chemical Analysis of Food

Techniques and Applications

Author: Yolanda Picó

Publisher: Academic Press

ISBN: 0123848628

Category: Science

Page: 798

View: 7127

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"The book contains twenty three chapters written by experts on the subject is structured in two parts: the first one describes the role of the latest developments in analytical and bioanalytical techniques, and the second one deals with the most innovative applications and issues in food analysis. The two first introductory chapters about sampling technique, from basic one to the most recent advances, which is still a food challenge because is responsible of the quality and assurance of the analysis, andon data analysis and chemometrics are followed by a review of the most recently applied techniques in process (on-line) control and in laboratories for the analysis of major or minor compounds of food. These techniques ranged from the non-invasive and non-destructive ones, such as infrared spectroscopy, magnetic resonance and ultrasounds, to emerging areas as nanotechnology, biosensors and electronic noses and tongues, including those already well-established in food analysis, such as chromatographic andelectrophoretic techniques. These chapters also include two important tools for solving problems in chemical and biological analysis such as mass spectrometry and molecular-based techniques"--
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NMR - From Spectra to Structures

An Experimental Approach

Author: Terence N. Mitchell,Burkhard Costisella

Publisher: Springer Science & Business Media

ISBN: 3540721967

Category: Science

Page: 207

View: 1052

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This practice-oriented textbook shows how to utilize the huge variety of NMR experiments available today in addition to standard experiments. Intended as a practical guide for students and laboratory personnel, it treats theoretical aspects only to the extent necessary to understand the experiments and to interpret the results. The book is significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems offers invaluable help for students, practitioners and laboratory personnel alike.
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NMR Spectroscopy Explained

Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology

Author: Neil E. Jacobsen

Publisher: John Wiley & Sons

ISBN: 9780470173343

Category: Science

Page: 640

View: 2615

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NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.
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Analytical chemistry

a modern approach to analytical science

Author: Jean-Michel Mermet,Matthias Otto,Robert Kellner

Publisher: Vch Verlagsgesellschaft Mbh

ISBN: 9783527305902

Category: Science

Page: 1181

View: 4901

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Why settle for less when you can have the whole of Analytical Chemistry in a single book? The successful all-in-one guide to modern Analytical Chemistry is now available in a new and updated edition. From the foundations of analytical science to state-of-the art techniques and instrumentation -- all you will ever need to know is explained here. The text covers both general analytical chemistry and instrumental analysis and may be used for most analytical chemistry courses offered today. Carefully chosen worked examples show how analytical problems can effectively be solved and how calculations should be performed. Study questions and recommended reading for further study are provided for each learning unit. The second edition has been carefully revised to keep up-to-date with advances in the technology of analytical methods in the laboratory and in the workplace, including newly written chapters on multidimensional chromatography, sensors and screening systems. With its broad scope, the text doubles as a reliable reference for virtually all analytical problems encountered during the course of study and beyond. "Analytical Chemistry will serve as an excellent text as well as a valued reference following completion of the student's course of study." Journal of Medicinal Chemistry "It is a book that should be on the shelves of all analytical chemistry and biochemistry professionals, including those who work in the areas of clinical chemistry, food chemistry and forensic chemistry." Bulletin of the World Health Organisation "The book is a must-have reference for anyone trying to understand what techniques and technologies are available for the analytical chemist today." Chemtech
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Optical Spectroscopy in Chemistry and Life Sciences

An Introduction

Author: Werner Schmidt

Publisher: Wiley-VCH

ISBN: 9783527299119

Category: Science

Page: 384

View: 3227

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This book is a compact and simultaneously comprehensive introduction to the theory and practice of optical spectroscopy. The author skillfully leads the reader from the basics to practical applications. The main topics covered are: - theory of optical spectroscopy - components of spectrometers (light sources, filters, lenses and mirror chromators, detectors, cuvettes) - evaluation of data and interpretation of spectra Such important methods as absorption and luminescence spectroscopy, scattering and reflection spectroscopy, photoaccustic spectroscopy, spectroscopy of atoms, polarimetry and near infrared spectroscopy are covered in depth. A useful appendix with the addresses of pertinent equipment manufacturers rounds off the work.
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Basic One- and Two-Dimensional NMR Spectroscopy

Author: Horst Friebolin

Publisher: Wiley-VCH

ISBN: 9783527312337

Category: Science

Page: 430

View: 8653

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This classic textbook for all users of NMR spectroscopy shows the basics of this technique and how to interpret the spectra. Covering the material taught in graduate courses, this text provides both students and professionals with a lucid introduction, thoroughly explaining the underlying theory but with a minimum of mathematics. Written by an NMR expert with long-standing teaching experience, this thoroughly enlarged and updated fourth edition includes - polymer solid state NMR - analysis of biopolymers - applications of magnetic resonance tomography and magnetic resonance spectroscopy. With its layout and illustrations designed for maximum clarity, this is a must for students and lecturers in chemistry, biochemistry, pharmacy, as well as spectroscopists. From reviews of previous editions: This book deserves much praise... The book forms an excellent bridge between the very simple texts on spectral interpreataion and more specialist works with an emphasis on mathematical theory... The many diagrams are clear and of high quality, and the examples of NMR spectra throughout the book are well chosen. This book is highly educational and will be of benefit to those who have to teach NMr and to students and scientists in academic and industrial laboratories who use NMR spectroscopy. NMR in Biomedicine 'This is an excellent book ... we have been using the first edition of the book in our graduate course in NMR for three years and have been very pleased with it. My opinion is that someone who began knowing nothing about NMR could become quite proficient at structure determination by simply mastering the contents of this book. I highly recommend it.' Journal of the American Chemical Society. 'Almost every course in chemistry and biochemistry nowadays has some NMR component, and the student's interest depends on how the material is delivered. This book is a pleasure to read and if it does not arouse the student's interest, then it is difficult to see what could. It is clearly written and illustrated, with a near perfect balance of mathematics and text.' Chemistry in Britain
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Practical organic synthesis

a student's guide

Author: Reinhart Keese,Martin Brändle

Publisher: Wiley

ISBN: 9780470029657

Category: Science

Page: 199

View: 1891

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Success in an experimental science such as chemistry depends on good laboratory practice, a knowledge of basic techniques, and the intelligent and careful handling of chemicals. Practical Organic Synthesis is a concise, useful guide to good laboratory practice in the organic chemistry lab with hints and tips on successful organic synthesis. Topics covered include: safety in the laboratory environmentally responsible handling of chemicals and solvents crystallisation distillation chromatographic methods extraction and work-up structure determination by spectroscopic methods searching the chemical literature laboratory notebooks writing a report hints on the synthesis of organic compounds disposal and destruction of dangerous materials drying and purifying solvents Practical Organic Synthesis is based on a successful course in basic organic chemistry laboratory practice which has run for several years at the ETH, Zurich and the University of Berne, and its course book Grundoperationen, now in its sixth edition. Condensing over 30 years of the authors’ organic laboratory teaching experience into one easy-to-read volume, Practical Organic Synthesis is an essential guide for those new to the organic chemistry laboratory, and a handy benchtop guide for practising organic chemists.
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